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INDIAN ARMY SEMINAR: EX GYANWARDHAN EQUIPMENT EXPOSITION, NEW DELHI

TRIBO-INDIA CONFERENCE ON TRIBOLOGY OF AUTOMOTIVE SYSTEMS, NEW DELHI

NEW FRONTIERS IN BIO FUELS:
DELHI TECHNOLOGY DEPARTMENT,
NEW DELHI


7TH INTERNATIONAL CONFERENCE
ON TRIBOLOGY FOR STEEL &
MINING INDUSTRIES, RANCHI

Model Rotroil

Model Rotroil is an optical emission spectrometer designed to determine the trace concentration in wear metals, polluting materials and additives in lubricating oils, transmission and refrigerating liquids. Determination of such components is very important in order to be able to make preventive maintenance and avoid the mechanical parts to break while in motion. The spectrometer is an highly precise and reliable product able to satisfy the demanding international rules. Rotroil spectrometer is produced both as lab and "in situ" instrument.
Model- COAT® System (Continuous Oil Analysis and Treatment)

Model- COAT® System (Continuous Oil Analysis and Treatment) is an analytical tool used for quality control, condition monitoring, and lubricant life extension that has revolutionised the way lubricating oils are monitored and maintained. When the eventual depletion of targeted additives falls below a predetermined limit, the COAT® System will alert the operator that the oil must be changed or a specific additive must be replenished. The maintenance of additive levels can be done manually or programmed automatically. The COAT® System uses Fourier Transform Infrared (FTIR) spectroscopy, integrated with a flow-through optical cell and product sampling system, all controlled through the powerful U.M.P.I.R.E software system running on a Windows computer.
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We offet difer-nt node of parSicl counter:

Model-PC-2200

Identifies Particle Quantity and Size from 0.5µm to 100µm diameter. Operates with both Flowing and In-situ Liquids. Utilizing the principle of "near angle light scatter", a revolving laser beam passes through the walls of a glass container of a flow-thru cell. When it is directed through a central "sensitive zone" the PC-2200 not only counts the particles in suspension, but tabulates their size as well. The analog signals generated by the light pulses are routed to a computer and digitized.
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Model-PC-2300

Measures Particle Quantity and Size from 0.5µm to 100µm diameter. AC or Battery operated, for both Insitu and Flowing Liquids, oil and water.
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Optical Emission Spectrometry is an analytical technique, universally considered and used to determine the chemical composition of metal alloys. Thanks to the method precision and the short analysis time, it represents a valid control system of production in all the fields regarding metal industry (primary alloys foundries, metal processing industries, mechanical industry) in any time during production cycle, in the case it is necessary to have a fast and accurate chemical analysis of material. We offer different model of OES:
1) Model - SOLARIS CCD PLUS(for metal)

Solaris CCD Plus spectrometer is the right instrument which combines ease of using, reliability and accuracy in results. Thanks to its reduced dimensions and to the quality of components, Solaris CCD Plus represents the ideal solution to be used in any working place: Office, Laboratory, Stock, production. Solaris CCD Plus is available with different configurations, able to analyze any different kind of metal alloys, ferrous and non ferrous ones.
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2) Model – ATLANTIS (for metal)


ATLANTIS is the new state of the art laboratory spectrometer for the best analysis and detection limits that allows evaluation of low concentrations (<1 ppm). ATLANTIS is a simultaneous multi-channel spectrometer specifically designed to analyze solid metallic samples granting at the same time superior analytical performance and easiness of use.
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3) Model-Solaris CCD NF


The work organization requires systematic, very thorough and fast checks of the production and incoming materials . Solaris CCD NF is an extremely useful tool for all the Quality oriented companies or a valid back-up instrument.Simple, fast and reliable, Solaris CCD NF is the ideal analyzer for: Small and medium foundries; Die casting foundries; Quality control of incoming materials Metal Trade and recycling Automotive industries
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4) ESA PORT (potable spectrometer)(for metals)


The optical emission portable spectrometer ESA PORT employs specifically dedicated CCD optical systems, which allow to offer a large analytical flexibility. The instrument is small sized and can be brought and used everywhere, from production department to warehouse. ESA PORT is an ideal instrument for PMI controls, for material sorting, for incoming and outcoming quality controls. The instrument is extremely functional and allows the rapid identification of all metal alloys and the analysis of elements such as C, Al, Si and Mg, etc. It is, for this reason, competitive to the portable X ray portable systems, because it has a bigger analytical capacity and is not submitted to restrictions related to radiogenic sources detection. At the moment all functions are regulated by PC and communications are made through optical fibres control system and using USB 2.0 technology. ESA PORT is powered by net current or can be linked to an external battery. A pratical and handy trolley makes it easy to be moved from a place to an other.
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X-ray diffraction (XRD) is a non-destructive technique for the qualitative and quantitative analysis of the crystalline materials, in form of powder or solid. Basically XRD is obtained as the "reflection" of an X-ray beam from a family of parallel and equally spaced atomic planes, following the Bragg's law. Many other investigations can be performed with the help of X-ray diffraction. Residual stress: With XRD it is possible to measure the strain (the deformation of the original lattice) and the stress is calculated thanks to the knowledge of the elastic constants of the material. Texture: it is the preferred orientation of the crystallites in a specimen. If a texture in a material is present, the intensity of a diffraction line changes with the orientation of the sample respect to the incident beam. Crystallite size and microstrain: These information are obtained by the analysis of the width and the shape of the diffraction lines. Structure analysis: XRD is used to investigate the crystallographic structure of a material. The position and the relative intensities of the diffraction lines can be correlated to the position of the atoms in the unit cell, and its dimensions. Indexing, structure refinement and simulation can be obtained with specific computer programs. Thin film: Keeping the incident beam at low angles, it is possible to investigate the properties of multilayers, minimising the interference of the substrate. On the same way, reflectometry can be performed. We offer different model of XRD:

1) APD 2000 PRO Diffractometer

It is an X-ray equipment for analyzing the structure of a material from the scattering pattern produced when an X-ray beam interacts with the sample. Powder diffraction is a technique used to characterize the crystallographic structure, crystallite size and orientation in polycrystalline or powdered solid samples. Powder diffraction is commonly used to identify unknown substances comparing diffraction data and it may also be used to characterize heterogeneous solid mixtures to determine relative abundance of crystalline compounds. APD 2000 PRO diffractometer is designed to be the best solution for phase and structural analysis of powder samples, using the well known Bragg-Brentano geometry. Fields of application include: environment, soil/rocks, clay, minerals, ceramic, cements, glasses, petroleum, catalyst, polymers, agricultural science, biosciences, chemicals, pharmaceuticals, cosmetics, forensic analysis.

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2) Model- Stress-X (Robotic Residual Stress Analyzer (Portable X-ray diffraction system)

Stress-X (Robotic Residual Stress Analyzer) allows to measure residual stress, providing a through non-destructive analysis of samples of any dimensions thanks to the original mounting of the Diffractometer head on a 6 anthropomorphic axis robot. The robot and the related measuring head are mounted on a robust trolley made of steel which holds all the control electronics, water cooler for X-ray tube cooling and personal computer
Robot allows accuracy in positioning and repeatability of 20 microns. It is possible to measure specimens positioned on the measuring platform on board or any other specimen positioned outside of the instrument basement at optimal measurement distance of 700 mm from the robot centre. Measurement target is defined by a combination of a Video camera for X-Y pointing and a laser for Z positioning. Laser accuracy is less of 10 microns with a measuring range of 300+/-70mm. Thanks to the 6 degree of freedom the measurement positions and angular ranges are practically unlimited.

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3) Model-The EXPLORER (High Resolution Diffraction System )

The EXPLORER high resolution diffraction system incorporates the high efficiency of the direct drive torque motors controlled by optical encoders, allowing to reach an angular accuracy of 0.00001°. Thanks to the modularity, all the hardware components can be changed allowing seven five independent degrees of freedom and investigations on a whole range of powders, bulk materials and thin layers. EXPLORER offers solutions for a wide range of analytical requirements, from routine crystalline phase identification and quantification, crystallite size/lattice strain and crystallinity calculations, retained austenite quantification, polymorph screening, crystal structures analysis, to residual-stress analysis, thin films, depth profiling, non-ambient analyses, phase transition, textures and preferred orientation, nanoparticles. The optics permit switches between Bragg-Brentano, focusing and parallel beam geometry using Johansson or parabolic mirror monochromators. The coupling between a parabolic mirror monochromator and a channel-cut crystal mounted on the incident beam allows to realise a monochromatic parallel beam with high intensity and low divergence, suitable for high resolution measurements.
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The radiation provided by a source of X-rays is allowed to fall on the sample to be analysed. The energy of the radiation must be sufficient to displace electrons in the K, L or M-shells of the atoms present in the sample.When an electron from the K-shells is displaced it leaves a vacancy which destabilises the energy structures of the atom.

An electron from a higher-energy level will fall into this vacancy. Such an electron can be provided by the L-shell, the energy associated with this transfer corresponds to that of the emission of a photon Ka with energy equal to the difference in energy possessed by electrons of the K and L shells. Such a transfer results also in a vacancy being created in the L-orbital which in turn is filled by transfer of an electron from the M-orbital, with emission of a photon L. This allows the atom to return to a more stable energy-state. The spectrum of wavelengths resulting from the energy-level-jumps of the electrons into the K-orbital is called the "K-series". Those originating in the L and M-orbitals are similarly called the "L and M series". For a given atom, the principal wavelength of each series has an intensity that is well defined and constant, subject to the laws of probability and to small variations which depend on the atomic number. The radiation emitted in these transitions appears in the X-ray part of the electromagnetic spectrum and is specific to each element in the periodic table. The energy of the emission is not influenced by the chemical bonding of the atom. The fluorescence effect is concerned only with the internal structure of the atom, and is not affected by the arrangement of the surrounding molecular orbitals. Using a solid-state detector it is now possible to detect all the elements in the periodic table from sodium to uranium simultaneously. By including a known quantity of a reference element in the sample, quantitative measurements of the other elements present can be obtained.

Model-TX 2000

TXRF is founded on the same principles of the EDXRF with, however, one significant difference. In contrast to EDXRF, where the primary beam strikes the sample at an angle of 45°, TXRF uses a glancing angle of a few milliradians. Owing to this grazing incidence, the primary beam is totally reflected. By illuminating the sample with a beam that is being totally reflected, absorption of the beam in the supporting substrate is largely avoided and the associated scattering is greatly reduced. This also reduced the background noise substantially. A further contribution to the reduction of the background noise is obtained by minimising the thickness of the sample. A small drop of the sample (5-100 microliters of the substance dissolved in an appropriate solvent) is placed on a silica carrier.On evaporation of the solvent a thin film, a few nanometers thick, remains. In practice the greater part of the scattering normally arising from the sample and its matrix is eliminated. This is because matrix effect cannot build up within minute residues or thin layers of a sample. Besides its high detection power, simplified quantitative analysis in made possible by internal standard.
X-Ray fluorescence
InfraLUM FT-10 is a multipurpose near-IR FT spectrometer designed for laboratory analysis of various samples, such food products as wheat, barley, rye, oats, wheat and rye flour, corn, soy beans and flour, soy oil meal, sunflower oil meal and cake, meat-and-bone meal tankage, fish flour, mixed fodder, feed yeast, dry milk, milk, curds, yogurts, cheese, minced meat, etc Most of the samples are analyzed without sample preparation. Preliminary grinding is necessary for some solid non-granular samples (e.g. soy and sunflower oil meal) or samples in highly absorbing coat (e.g. sunflower seeds). InfraLUM FT-10 is designed in such a way to simplify sample preparation and increase accuracy of the analysis as much as possible.
Near –IR FT
InfraLUM WholeGrain Analyzer is a near-IR FT spectrometer designed for laboratory analysis of basic properties/constituents of grain, such as protein, fats, moisture, sugar, cellulose, starch, fibres, etc. The instrument employs the NIR-transmission technique, accommodates most of chemometrics prediction algorithms, and allows for high flexibility of analysis methods. The analyzer provides very simple user interface via dedicated SpectraLUM/Pro®software and touchscreen, which enables to carry out routine analyses in a dialogue mode, so that an operator can operate the instrument without any special training. The most precise FT spectrometry together with potion wise sampling ensures most accurate results that can be obtained by NIR spectrometry. WHOLEGRAIN NIR


High performance capillary electrophoresis. Based on the differential migration of components of aqueous samples within a narrow quartz capillary under the influence of the applied electric field. Separated solutes are quantitatively detected at the capillary outlet by high sensitive optical system based on direct or indirect UV absorbance. We offer different models for Capillary Electrophoresis
1) MODEL-CAPEL®-103RT CAPILLARY ELECTROPHORESIS SYSTEM

Capel-103RT is a basic capillary electrophoresis system with manual sampling and single wavelength photometric detector that is ideal for educational purposes. The system has liquid cooling of capillary that improves the reproducibility of analysis.
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2) MODEL-CAPEL®-105 CAPILLARY ELECTROPHORESIS SYSTEM

Capel-105 is an advanced capillary electrophoresis system with an autosampler that allows fast and effective solution for food industry, environmental applications, pharmaceutical and chemical industries, biochemistry, forensic science
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3) CAPEL-105M CAPILLARY ELECTROPHORESIS SYSTEM

It is an advanced capillary electrophoresis system with an autosampler that allows fast and effective solution for food industry, environmental applications, pharmaceutical and chemical industries, biochemistry, forensic science.
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The fluorescence (phosphorescence, chemiluminescence) intensity measurement and measurement of transmittance of a sample

1) MODEL-FLUORAT®-02-SERIES LIQUID ANALYZERS

FLUORAT-02 have gained a wide use in many analytical laboratories, makes a base for a large number (more than 50 certified methods) of analytical fluorometric, photometric,and chemoluminometric techniques for analysis of water, food, emission analysis. Such a versatility allows an analyst to choose the optimal method for assaying each component being determined. The Fluorat analyzers embody the modular principle. The base unit FLUORAT-02-3M is a filter fluorimeter, chemiluminometer and photometer implemented together in the same optoelectronic scheme, whereas the FLUORAT-02-2M version is, in addition, a time-resolving fluorimeter and can also be used as a fluorimetric detector in any HPLC system, relevant measuring cells being interchangeable. FLUORAT-02 is an automated analyzer furnished with a package of certified methods for monitoring the quality of drinking and waste water in compliance with sanitary regulations, as well as for assaying a number of air, soil, and food product constituents. The analytical methods implemented using this instrument are chosen so that to reliably detect half of the prescribed UTC and to provide the simplest sample preparation. For example, it takes 2 to 3, 5 to 7, and 2 to 3 minutes, respectively, to prepare a sample of petroleum hydrocarbons, phenols, and surfactants for analysis.
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2) Model-FLUORAT®-02-PANORAMA SPECTROFLUOROMETER

FLUORAT-02-PANORAMA spectrofluorometer is the most sophisticated instrument among the FLUORAT-02 family. It is intended for scientific research, chromatographic analysis, and for operation as part of multimodule automatic measuring facilities. The spectral regions in the excitation and detection cahnnels are set by built-in fast monochromators. The monochromators are controlled independently, so that the analyst can program any of their operation functions in the process of measuring, in particular, the spectra can be synchronously scanned. A proprietary optical scheme provides the high sensitivity of the instrument, especially in the UV spectral range, where the isolation of a spectral interval using a light filter is difficult.The instrument is controlled either from a built-in keypad or from an external Computer

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Is based on the effect of light scattering by suspended particles or emulsions

1) MODEL-MICROPARTICLE CONCENTRATION ANALYZER CKAT-1

CKAT-1 analyzer is designed for continuous automatic monitoring of content of suspended particles and petroleum products in water samples (turbidity measurements) and for monitoring of water color. Analyzer performs automatic monitoring of water stream for technological processes of water treatment, power generation industry, for environmental monitoring. The analyzer does not consume any chemicals during measurement. The analyzer may be incorporated in a complex control system of water treatment process.The analyzer has several modifications that are customized for different applications: «CKAT-1» for analysis of suspended particulate matter in the range of 50 - 50 000 mg/l. Main application – monitoring of discharge water at the mining industry. «CKAT-1» measures the content of suspended particles in water in the range of 0.1 - 50 mg/l. There exist two modifications of the instrument – for measurements of low concentrations and the instrument with non-contaminated cell.«CKAT-1» modification of the analyzer measures the water color

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2) MODEL-FLUORAT® AE-2 OIL-IN-WATER ANALYZER

Fluorat AE-2 analyzer is designed for continuous automatic monitoring of content of petroleum hydrocarbons in potable, natural, and waste water. The instrument comprises a sample preparation unit and a FLUORAT®-type luminescence detector. The sample preparation unit provides metered water feed and switching of the water and reagent flows, control of temperature, mixing and mass-exchange processes. The detector (or optical cell) performs the detection of luminescence of petroleum hydrocarbons extracted by hexane from the sample using a patented chromato membrane technology. A special modification of the instrument Fluorat AE-2C modification is designed for monitoring of the waste water or natural waters with high risks of contamination. The analyzer is installed stationary and is controlled using a built-in microprocessor or an external PC. In a stand-alone operating mode, the selected reaction sequence can be assigned from a built-in keyboard.Concentration measurement results, are stored in a built-in memory and are displayed, in milligrams per liter, on a built-in digital LC display. If concentration of petroleum hydrocarbons exceeds a threshold level, the alarm mode is activated and a relay may be triggered following a command from the analyzer.
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3) WATER HARDNESS ANALYZER AKMS-1

AKMC-1 analyzer is designed for continuous automatic monitoring of total content of calcium and magnesium salts (total hardness) in water. Analyzer performs automatic monitoring of water stream for technological processes of water treatment, power generation industry, for environmental monitoring. The analyzer does not consume any chemicals during measurements. The analyzer may be incorporated in a complex control system of water treatment process
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